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NBT assay

Contributor: Suprya Jayadev
Date: January 10, 1991



NBT solution
1.5 mls - PBS
3 mg - NBT powder
3 µl - 0.162 mM TPA (stock 1 mg/ml; 1.62 mM)

Procedure

1) Spin ~1 ml of cells at 1500 rpm for 5 mins.

2) Resuspend pellet in 100 µl PBS + 100 µl NBT solution.

3) Incubate in 370C water bath for 1 hour.

4) Stop reaction with 3 ml ice cold PBS.

5) Spin at 1500 rpm for 5 mins.

6) Resuspend in 200 µl PBS and load 100 µl into slide chamber.

7) Spin at 3000 rpm for ~1 min.

8) Allow slides to dry.

9) Fix with methanol - 1 minute.

10) Rinse with water.

11) Counterstain with Safranin-O - 1.5 mins.

12) Rinse off excess stain.

13) Allow slides to dry and count cells.